FIELD: production of super pure material. SUBSTANCE: powder of silicium carbide is fed into fluoroplastic reactor and poured by mixture of 7.5-12.5 M nitric acid and hydrofluoric acid, volume ratio of said acids being 1: (3-5) respectively. Then heating and boiling within 2.5-3 h followed by washing with distilled water and by annealing are carried out. Said annealing takes place on open air within 1.5-2 h at 1.5-2 h. Desired material contains 0.3 •10-4-10-3 % of SiO2, and not more 0,05•10-4 % of free silicium and carbon. EFFECT: improves efficiency of method. 1 tbl
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Authors
Dates
1996-05-27—Published
1992-02-25—Filed