FIELD: analytical chemistry. SUBSTANCE: invention is intended for use in spectral and other methods of analytical chemistry, predominantly while analyzing highly pure substances and materials, specifically in manufacture of semiconductor materials and fibre-optical light guides. Device is inserted with element of precipitation and secondary fraction sublimation of volatile reagent in closed space in which highly pure substance and volatile reagent for its disintegration are positioned separately during analysis of microimpurities. EFFECT: enhanced efficiency and accuracy of device. 4 cl, 2 dwg
Authors
Dates
1997-04-27—Published
1994-05-10—Filed