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Application

96123869/04, 1996-12-24

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Actual filing date

1996-12-24

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Published

1998-01-20

(72)

Inventor

Zheludov E.A.Seljakov B.A.Suchkova O.V.Ul'Jantsev M.A.

(73)

Holder

Otkrytoe Aktsionernoe Obshchestvo Dzerzhinskij Opytnyj Zavod Aviatsionnykh Materialov

METHOD FOR PRODUCING DIETHYLMETHOXY BORANE Russian patent published in 1998 - IPC

Abstract RU 2102397 C1

FIELD: organic chemistry; production of organoboron compounds, particularly, esters of dialkyl boric acids, namely, production of diethylmethoxy borane. SUBSTANCE: method involves interaction of triethyl borane and methyl alcohol in the presence of pivalic acid which takes place at 2-10 C. Molar ratio of triethyl borane, methanol and pivalic acid is 1:(1.005-1.01): 0.005-0.01, respectively. Reaction mass is allowed to stand at 18-22 C, and product is isolated by rectification. Yield of product is 93-94 %, its degree of purity is 99.9 %. Diethylmethoxy borane may be used together with sodium boron hydride by diastereoselective reduction of β-hydroketones into 1,3-dioles. EFFECT: improved efficiency.

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RU 2 102 397 C1

Authors

Zheludov E.A.

Seljakov B.A.

Suchkova O.V.

Ul'Jantsev M.A.

Dates

1998-01-20—Published

1996-12-24—Filed

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