METHOD OF PREPARING ALFA-BROMOISOVALERIANIC ACID ETHYL ESTER Russian patent published in 1998 - IPC

Abstract RU 2111954 C1

FIELD: organic chemistry, more particularly pharmaceutical industry. SUBSTANCE: claimed method comprises preparing alphabromoisovalerianic acid by direct bromination of isovalerianic acid with bromine in the presence of small amounts of chloride-containing agents such as phosphorus trichloride, phosphorus oxychloride, thionyl chloride, isovalerianic acid chloride and subsequently esterifying the resulting acid with ethanol. Yield of the desired product is 92.4%. EFFECT: more efficient preparation method. 1 tbl

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RU 2 111 954 C1

Authors

Tsukanov I.A.

Antonova N.N.

Ehl'Man A.R.

Kurlaev V.V.

Zarytovskij V.M.

Dates

1998-05-27Published

1996-09-27Filed