METHOD OF PREPARING 5H-DIBENZ (b,f) AZEPIN-5-CARBOXAMIDE Russian patent published in 1999 - IPC

Abstract RU 2124504 C1

FIELD: therapy. SUBSTANCE: claimed method comprises reacting iminostilbene with alkaline cyanate in acetic acid, in acetic acid-water or acetic acid-alcohol mixtures. Acetic acid-water mixture comprises up to 20 wt % and acetic acid-alcohol comprises up to 10 wt % methanol or ethanol. Alkaline cyanate such as sodium or potassium cyanate in the form of aqueous solution is added gradually to reaction mixture. The claimed method makes it possible to simplify process. EFFECT: more efficient preparation method. 7 cl, 7 ex

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RU 2 124 504 C1

Authors

Rudol'F Ehkardt

Khans-Joakhim Ensh

Dates

1999-01-10Published

1994-07-21Filed