FIELD: chemical industry. SUBSTANCE: corresponding derivatives of azamacrocyclic or acyclic aminophosphonates which contain at least one secondary or primary nitrogen atom substituted by at least one fragment of formula: -CH2PO3RR1 (I), wherein R is C1-5 alkyl, hydrogen, Na or K are prepared by reacting corresponding unsubstituted amine with strialkyl phosphite and para-formaldehyde followed by aqueous alkaline hydrolysis to obtain derivatives substituted by fragment of formula I. Method makes it possible to prepare the desired compound with yield of at least 90%. EFFECT: more efficient preparation method. 34 cl, 18 ex
Title |
Year |
Author |
Number |
COMPLEXES OF METALS WITH BICYCLOPOLYAZAMACROCYCLE, METHOD OF THEIR SYNTHESIS AND A PHARMACEUTICAL COMPOSITION USED FOR TREATMENT OF PATIENTS WITH CANCER |
1992 |
- Gehrri E.Kifer
- Dzhejm Sajmon
|
RU2118325C1 |
DERIVATIVES OF BICYCLOPOLYAZAMACROCYCLOPHOSPHONIC ACIDS OR THEIR PHARMACEUTICALLY ACCEPTABLE SALTS AND A METHOD OF THEIR SYNTHESIS |
1992 |
- Gehrri E.Kifer
- Dzhejm Sajmon
- Dzhozef R.Garlik
|
RU2114115C1 |
METALLOCOMPLEXES CONTAINING SUBSTITUTED INDENYL AND METHOD OF POLYMERIZATION OF OLEFINS |
1996 |
- Piter N. Nikias
- Mark Kh. Makadon
- Dzhehsson T. Patton
- Bernard P. Fridrikhsen
- Jorge Soto
- Dzhejms S. Stivens
- Dehniel' D. Vanderlende
|
RU2175325C2 |
METAL CHELATES COMPRISING LIGANDS OF 3-ARYL-SUBSTITUTED INDENYL, CATALYST OF OLEFIN POLYMERIZATION AND METHOD OF POLYMERIZATION |
1997 |
- Nikias Piter N.
- Patton Dzhesson T.
|
RU2186073C2 |
METHOD OF PURIFICATION OF ETHYLENEDIAMINOTETRA(METHYLENEPHOSPHONIC ACID) OR 1,4,7,10-TETRAAZACYCLODODECANE-1,4,7,10-TETRA(METHYLENEPHOSPH- ONIC ACID) |
0 |
- Dzhozef R. Garlich
- Dzhejms Sajmon
- Tipton T. Masterson
|
SU1838321A3 |
METAL CHELATE AND METHOD OF OLEFIN POLYMERIZATION |
1997 |
- Klozin Ezhi
- Kruper Vill'Jam Dzh. Ml.
- Nikias Piter N.
- Patton Jasson T.
- Vil'Son Dehvid R.
|
RU2196776C2 |
NEW GADOLINIUM CHELATE COMPOUNDS WITH HIGH RELAXIVITY FOR USE IN MAGNETIC RESONANCE IMAGING |
2017 |
- Berger Markus
- Lohrke Jessica
- Hilger Christoph-Stephan
- Jost Gregor
- Frenzel Thomas
- Panknin Olaf
- Pitsch Hubertus
|
RU2755181C2 |
TITANIUM(II) AND ZIRCONIUM(II) COMPLEXES, CATALYTIC COMPOSITION, AND METHOD OF POLYMERIZATION OF ETHYLENICALLY UNSATURATED OLEFINS |
1994 |
- Dehvid D.Divor
- Linore Kh.Kroford
- Dzhejms S.Stivens
- Fransiz Dzh.Timmers
- Robert D.Massel
- Dehvid R.Vilson
- Robert K.Rouzen
|
RU2135509C1 |
COMPLEX BICYCLOPENTADIENYLDIENE COMPOUNDS AND METHOD OF POLYMERIZATION OF OLEFINS |
1995 |
- Frehnsis Dzh.Timmers
- Dehvid D.Devour
- Dzhejms S.Stivens
- Robert K.Rozen
- Dzhehsson T.Pehtton
- Dehvid R.Nejtemer
|
RU2135508C1 |
COMPOUNDS FOR SEPARATION OF REAR EARTH ELEMENTS AND S-, P-, D-METALS, SEPARATION METHODS, AND THEIR USE |
2018 |
|
RU2783526C2 |