FIELD: organic chemistry. SUBSTANCE: method is carried out by reacting tetrafluoroethylene with mixture of iodine and iodine pentafluoride at temperature of 40-80 C in the presence of metallic antimony as catalyst and in the presence of mixture of difluoromethane with trifluoroethylene in amount of 7•10-4÷2,6•10-2 wt %. Process efficiency becomes higher, no inert diluent is used, process becomes cheaper and is less dangerous, and final product having high content of main agent is obtained, and additional purification thereof is thus avoided. EFFECT: more efficient preparation method.
Title | Year | Author | Number |
---|---|---|---|
METHOD OF IODOFLUOROALKANE SYNTHESIS | 1993 |
|
RU2064915C1 |
METHOD OF PRODUCING PENTAFLUOROIODOETHANE | 2017 |
|
RU2642789C1 |
METHOD OF SYNTHESIS OF ADDUCTS OF FLUORO-CONTAINING HYDROCARBONS AND OLEFINS | 1997 |
|
RU2181114C2 |
METHOD OF SYNTHESIS OF POLYFLUORINATED ALCOHOLS | 1999 |
|
RU2150459C1 |
METHOD OF PREPARING HEXAFLUOROETHANE | 1999 |
|
RU2155179C1 |
TETRAFLUOROETHYLENE PRODUCTION PROCESS | 2000 |
|
RU2167847C1 |
METHOD FOR PREPARING POLYFLUORINATED ALCOHOLS | 2002 |
|
RU2209204C1 |
METHOD OF PREPARING EMULSIFIER BY DISPROPORTIONATION OF UNSATURATED ACIDS | 2001 |
|
RU2174994C1 |
0 |
|
SU429590A3 | |
METHOD FOR PRODUCTION OF POLYFLUORINATED ETHERS | 2002 |
|
RU2203881C1 |
Authors
Dates
2000-01-10—Published
1999-07-20—Filed