METHOD OF SYNTHESIS OF 3,5-DINITRO-1,2,4-TRIAZOLE SALTS Russian patent published in 2001 - IPC

Abstract RU 2174120 C1

FIELD: organic chemistry, chemical technology. SUBSTANCE: synthesis of 3,5-dinitro-1,2,4-triazole salts is carried out by interaction of alkaline metal carbonates or hydrocarbonates with 3,5-dinitro-1,2,4-triazole solution in acetone. To synthesize 3,5-dinitro-1,2,4- triazole hydrazine hydrate, hydrochloric acid and dicyanodiamide are heated in the mole ratio 1:2:1 and temperature 45-50 C and formed solution is poured to sodium nitrite an aqueous solution at 40-50 C at vigorous stirring. Invention can be used in production of biologically active compounds and nitro-derivatives of 1,2,4-triazole used in different fields. EFFECT: decreased cost of process, enhanced safety of process. 2 tbl, 4 ex

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RU 2 174 120 C1

Authors

Chernyshev V.M.

Zemljakov N.D.

Taranushich V.A.

Dates

2001-09-27Published

2000-03-07Filed