METHOD OF SYNTHESIS OF METHYLSILANE Russian patent published in 2002 - IPC

Abstract RU 2177946 C1

FIELD: organic chemistry, chemical technology. SUBSTANCE: invention describes method of synthesis of methylsilane that involves reduction of methyl- dichlorosilane with lithium- aluminium hydride in medium of high-boiling ether of the formula (CnH2n+1)2O where n = 4-7 in the excess of lithium-aluminium hydride 5-10 wt. -% of stoichiometric amount and reaction is carried at temperature 30-50 C. EFFECT: simplified method of process, excluded purification stage. 4 ex

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RU 2 177 946 C1

Authors

Storozhenko P.A.

Shutova O.G.

Kuznetsova V.N.

Kozhevnikov B.E.

Sidorov D.V.

Chernyshev E.A.

Dates

2002-01-10Published

2000-12-18Filed