FIELD: analytical methods. SUBSTANCE: process and product quality control in production of chloral is accomplished as follows: sample to be analyzed is passed in gas carrier flow through chromatographic column filled with Polysorb-1 modified with polymethylsiloxane liquid used in amount 1.3-1.5 mg per 1 sq.m of Polysorb surface. For analysis, industrial-grade chloral or chloral rectification fractions are taken, whereas impurities are registered with the aid of heat-conductance detector. Water, ethanol, and dichloroacetal are simultaneously determined in mixtures also containing acetaldehyde and organochlorine compounds. EFFECT: expanded analytical possibilities. 3 cl, 3 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR GAS CHROMATOGRAPHIC DETERMINATION OF SULFUR FLUORIDES | 1999 |
|
RU2160896C1 |
METHOD OF GAS-CHROMATOGRAPHIC DETERMINATION OF PERFLUOROISOBUTYLENE | 2001 |
|
RU2189037C1 |
TECHNIQUE OF GAS-CHROMATOGRAPHIC DETERMINATION OF NITROGEN LOWER OXIDE IN GASES | 2003 |
|
RU2226688C1 |
GAS CHROMATOGRAPHIC METHOD FOR DETERMINING FLUOROHYDROCARBONS | 2002 |
|
RU2231058C1 |
METHOD OF IDENTIFYING AND DETERMINING WEIGHT CONCENTRATION OF ACETALDEHYDE IN ALCOHOL-CONTAINING SOLUTIONS | 1999 |
|
RU2162599C1 |
1,1-DIFLUOROETHANE PRODUCTION PROCESS | 1997 |
|
RU2150452C1 |
METHOD OF PURIFYING 1,1,1-FLUORODICHLOROETHANE | 1998 |
|
RU2157362C2 |
DIFLUOROCHLOROMETHANE PRODUCTION PROCESS | 2000 |
|
RU2180654C1 |
METHOD OF ISOLATING CHLORAL | 1999 |
|
RU2160247C1 |
METHOD FOR SIMULTANEOUS PREPARING CHLOROFORM AND SODIUM FORMATE | 2002 |
|
RU2222521C1 |
Authors
Dates
2003-10-27—Published
2002-09-19—Filed