FIELD: analytical methods. SUBSTANCE: invention, in particular, relates to determining quantitative and individual composition of organochlorine compounds in crude oils, petroleum processing products, and chemical reagents in petroleum production and petroleum processing industries. Mixture to be analyzed is passed with gas carrier stream through evaporator at 220-350 C, separated in capillary column of chromatograph at 50 to 320 C, and detected at 220-350 C in electron-acceptor detector, into which gas carrier is additionally forced at flow rate 200 cu.cm/min, whereupon, from quantitative and individual composition of organochlorine compounds, particular contamination source is found out. EFFECT: lowered detection threshold and increased determination accuracy. 2 cl, 1 tbl
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR DETERMINATION OF ORGANOCHLORINE COMPOUNDS IN OIL AND PETROLEUM PRODUCTS BY CHROMATOGRAPHIC METHOD | 2020 |
|
RU2748390C1 |
METHOD OF PREPARING SAMPLES OF OIL-FIELD CHEMICALS FOR DETERMINING ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE | 2019 |
|
RU2713166C1 |
METHOD FOR DETERMINING THE MASS CONCENTRATIONS OF ORGANOCHLORINE COMPOUNDS IN CHEMICAL REAGENTS USED IN THE PROCESS OF EXTRACTION, PREPARATION AND TRANSPORTATION OF OIL | 2022 |
|
RU2792016C1 |
METHOD FOR DETERMINING CONTENT OF ORGANOCHLORINE COMPOUNDS IN AN OIL SAMPLE AND INSTALLATION FOR ITS IMPLEMENTATION | 2023 |
|
RU2809978C1 |
METHOD FOR IDENTIFICATION AND QUANTITATIVE DETERMINATION OF ORGANOCHLORINE COMPOUNDS | 2021 |
|
RU2779701C1 |
SAMPLING DEVICES OF CONTINUOUS AND CYCLIC TYPE AND METHOD FOR DETECTING MIXTURE COMPONENTS USING SAMPLING DEVICES | 2020 |
|
RU2745752C1 |
METHOD OF DETERMINING VOLATILE PHYTONCIDES | 2012 |
|
RU2502994C1 |
METHOD FOR DETERMINING THE CONTENT OF ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE IN CHEMICAL REAGENTS AND EVALUATING THE EFFECT OF CHEMICAL REAGENTS ON THE FORMATION OF ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE IN OIL | 2021 |
|
RU2763683C1 |
METHOD FOR PREPARING SAMPLES OF OILFIELD CHEMICAL REAGENTS FORMING WATER-HYDROCARBON EMULSIONS AND WATER-HYDROCARBON EMULSIONS FOR THE DETERMINATION OF ORGANOCHLORINE COMPOUNDS AND ORGANICALLY BOUND CHLORINE | 2020 |
|
RU2743205C1 |
METHOD FOR PREPARATION OF SAMPLES OF OIL FIELD CHEMICALS FOR DETERMINATION OF ORGANIC CHLORINE COMPOUNDS AND ORGANICALLY BINDED CHLORINE | 2020 |
|
RU2746648C1 |
Authors
Dates
2003-12-20—Published
2002-07-25—Filed