FIELD: industrial organic synthesis.
SUBSTANCE: method is accomplished by drying and then calcining uranium tetrafluoride in rotary tubular furnaces constituting assembled system provided with ventilation system, cooling screw, and container. Heat treatment of product is effected in air-completed own gas atmosphere, formation of atmosphere including calcination step gases. Air is preheated to 300-400°C and fed in countercurrent mode at a rate of 2-8 m3/h into calcination step and at 100-250 m3/h into drying step. Anhydrous product is cooled to 180°C or below and tightly sealed in container.
EFFECT: reduced power and materials consumption.
5 cl, 2 tbl
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Authors
Dates
2005-07-27—Published
2003-08-07—Filed