METHOD FOR PREPARING SYNTHETIC GUTTA-PERCHA (VARIANTS), SYNTHETIC GUTTA-PERCHA (VARIANTS) AND COMPOSITION FOR TIGHT MEDICINAL BANDAGE (VARIANTS) Russian patent published in 2006 - IPC C08F36/08 C08F136/08 C08L9/00 A61L15/07 A61L15/12 

Abstract RU 2274644 C2

FIELD: medicine, chemical technology.

SUBSTANCE: invention relates to a method for preparing polyisoprene trans-isomers and for preparing materials of medicinal designation also. The polymerization reaction of isoprene is carried out in aliphatic solvent medium in the presence of a catalyst applied or not applied on silica gel. Catalyst represents titanium tetrachloride precipitated on magnesium dichloride. The polymerization reaction is carried out at 25-40°C, at the concentration of isoprene in the polymerization medium 0.8-1.0 mole/l, in the mole ratio co-catalyst : catalyst from 32 to 50. By other variant the polymerization reaction of isoprene is carried out in gaseous phase at 18-25°C with preliminary pre-polymerization. Prepared synthetic gutta-percha is used, in particular, as a binding agent in combination with dispersed mineral filling agent in composition for the tight medicinal bandage. Invention provides enhancing hardness of gutta-percha and decreasing hardening time of the composition.

EFFECT: improved preparing method.

9 cl, 1 tbl, 9 ex

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RU 2 274 644 C2

Authors

Antipov Evgenij Mikhajlovich

Karpov Oleg Pavlovich

Mushina Evgenija Aronovna

Petrushanskaja Nonna Veniaminovna

Podol'Skij Jurij Jakovlevich

Smetannikov Oleg Vladimirovich

Surovtsev Anatolij Aleksandrovich

Frolov Vadim Mikhajlovich

Chinova Marija Sergeevna

Dates

2006-04-20Published

2004-04-08Filed