METHOD FOR PREPARING DI-[(6-BENZYL-4,2,6-THIADIAZOLIDINE-2-YL)METHYL]SULFIDE Russian patent published in 2007 - IPC C07D417/12 

Abstract RU 2305098 C1

FIELD: organic chemistry, organic synthesis, chemical technology.

SUBSTANCE: invention describes a method for synthesis of di-[(6-benzyl-4,2,6-thiadiazolidine-2-yl)methyl]sulfide of the general formula (1): . Method involves interaction of formaldehyde aqueous solution saturated with hydrogen sulfide with benzyl hydrazine in the mole ratio benzyl hydrazine : formaldehyde : hydrogen sulfide = 1:3:2, respectively, at temperature 0°C and stirring the mixture for 3 h. Invention provides preparing the end product with high regioselectivity.

EFFECT: improved method of synthesis.

1 cl, 1 ex

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RU 2 305 098 C1

Authors

Akhmetova Vnira Rakhimovna

Nadyrgulova Guzel' Razhapovna

Khafizova Svetlana Rinatovna

Kunakova Rajkhana Valiullovna

Tjumkina Tat'Jana Viktorovna

Dzhemilev Usein Memetovich

Dates

2007-08-27Published

2006-01-31Filed