FIELD: organic chemistry, organic synthesis, chemical technology.
SUBSTANCE: invention describes a method for synthesis of di-[(6-benzyl-4,2,6-thiadiazolidine-2-yl)methyl]sulfide of the general formula (1): . Method involves interaction of formaldehyde aqueous solution saturated with hydrogen sulfide with benzyl hydrazine in the mole ratio benzyl hydrazine : formaldehyde : hydrogen sulfide = 1:3:2, respectively, at temperature 0°C and stirring the mixture for 3 h. Invention provides preparing the end product with high regioselectivity.
EFFECT: improved method of synthesis.
1 cl, 1 ex
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Authors
Dates
2007-08-27—Published
2006-01-31—Filed