ORGANOSILICA PREPARATION METHOD Russian patent published in 2007 - IPC C01B33/16 C09C1/28 C09C3/08 C07F7/02 

Abstract RU 2309120 C1

FIELD: silicon compounds.

SUBSTANCE: invention is related to preparation of silicas modified with organic and organosilicon compounds. Organosilica preparation method comprising synthesis of silica from silicon tetrachloride, cooling synthesis products, precipitating silica from synthesis products, additionally purifying silica with inert gas to remove gaseous synthesis products, modifying silica with organic or organosilicon compounds by way of treating silica with vapors of indicated compounds mixed with inert gas, precipitating thus formed organosilica from modification products, and additionally purifying organosilica with inert gas to remove gaseous modification products is characterized by that synthesis of silica is accomplished by oxidation of silicon tetrachloride with oxygen at 1000 to 2100°C and silicon tetrachloride-to-oxygen molar ratio between 1.0 and 3.0.

EFFECT: enhanced efficiency of and simplified organosilica preparation procedure.

4 cl, 1 tbl

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RU 2 309 120 C1

Authors

Gorovoj Mikhail Alekseevich

Gorovoj Jurij Mikhajlovich

Kljamko Andrej Stanislavovich

Pranovich Aleksandr Aleksandrovich

Vlasenko Viktor Ivanovich

Korzhakov Vladimir Viktorovich

Dates

2007-10-27Published

2006-08-17Filed