FIELD: organic chemistry, chemical technology.
SUBSTANCE: invention relates to a novel method for synthesis of N-phosphonomethylglycine. Method involves interaction of hexahydrotriazine compound with triacyl phosphite in organic solvent, saponification of formed phosphonic compound after preliminary extraction into aqueous phase, separation of organic phase and precipitation of N-phosphonomethylglycine by pH value control in the range from 0.5 to 2.0. Invention prevents decomposition of an organic solvent in saponification.
EFFECT: improved method of synthesis.
8 cl, 3 tbl, 4 ex
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Authors
Dates
2007-11-27—Published
2002-06-21—Filed