FIELD: chemical technology.
SUBSTANCE: method for synthesis of threadlike aluminum nitride involves passing gaseous reagents as aluminum (III) halides and nitrogen through heated aluminum and the following condensation of the end product. Aluminum (III) halide is fed at the level rate 0.1-6 cm3/min per 1 cm2 of the condensation surface. Condensation is carried out on backing made of pure graphite. Invention provides synthesis of aluminum nitride as crystal fibers showing the ratio value of length to diameter above 200-300. Invention can be used for synthesis of threadlike aluminum nitride crystals useful in making sensor probes in cantilevers of atomic-power microscopes.
EFFECT: improved method of synthesis.
3 dwg, 2 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR PRODUCING ALUMINIUM NITRIDE WHISKERS | 2016 |
|
RU2617495C1 |
METHOD OF MANUFACTURING THREAD-LIKE ALUMINUM NITRIDE | 1996 |
|
RU2106298C1 |
METHOD OF PRODUCING SUBMICRON CRYSTALS OF ALUMINIUM NITRIDE | 2019 |
|
RU2738328C2 |
METHOD FOR PREPARING ALUMINUM NITRIDE POWDER | 2005 |
|
RU2312060C2 |
METHOD OF PRODUCING DISPERSED ALUMINIUM NITRIDE, INSTALLATION AND REACTION CHAMBER FOR ITS IMPLEMENTATION | 2015 |
|
RU2638975C2 |
METHOD OF PREPARING ALUMINIUM NITRIDE | 1995 |
|
RU2074109C1 |
GROWTH OF GaN NANOTUBES, ACTIVATED WITH Si DOPANT ON Si SUBSTRATES WITH THIN AIN BUFFER LAYER | 2016 |
|
RU2711824C1 |
METHOD OF PRODUCING MOULDED ALUMINIUM OXYNITRIDE IN BURNING MODE | 2008 |
|
RU2370472C1 |
METHOD OF PRODUCING ALUMINIUM NITRIDE | 2010 |
|
RU2428376C1 |
REACTION INSTALLATION CAMERA FOR PRODUCING DISPERSED ALUMINIUM NITRIDE | 2014 |
|
RU2631076C2 |
Authors
Dates
2007-12-10—Published
2006-04-25—Filed