METHOD OF OBTAINING 3,5-DIAMINO-6-(2,3-DICHLORPHENYL)-1,2,4-TRIAZINE OF HIGH PURITY GRADE Russian patent published in 2008 - IPC C07D253/75 C07C281/16 

Abstract RU 2335497 C2

FIELD: chemistry.

SUBSTANCE: invention claims a new method of obtaining 3,5-diamino-6-(2,3-dichlorphenyl)-1,2,4-triazine of high purity degree by reaction of 2,3-dichlorbenzoylcyanide with 1-2 mol equivalents of dimethylase aminoguanidine salt in the presence of 3-6 mol equivalents of methanesulfoacid, with further addition of 2-5 mol equivalents of magnesium oxide to the reaction mix. The process is performed at 50-80°C, and target product is recrystallised from acetone.

EFFECT: improved efficiency of compounds.

5 cl, 3 ex

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RU 2 335 497 C2

Authors

Neu Jozhef

Gizur Tibor

Terli Jozhef

Chabai Janosh

Veg Ferents

Kal'Vin Peter

Tarkan'I Gabor

Dates

2008-10-10Published

2003-09-18Filed