METHOD OF OBTAINING PALLADIUM CATALYST ON ACTIVE ALUMINIUM OXIDE FOR LOW-TEMPERATURE CARBON OXIDE OXIDATION Russian patent published in 2008 - IPC B01J23/44 B01J23/755 B01J37/02 B01J21/04 B01D53/62 

Abstract RU 2339446 C1

FIELD: chemistry.

SUBSTANCE: invention relates to field of production of catalysts, containing porous carrier (active aluminium oxide) and deposited on it catalytically active metal (palladium) for low-temperature oxidation of carbon oxide and can be used in means of individual and collective protection of respiratory organs of people. Described is method of obtaining palladium catalyst on active aluminium oxide for low-temperature oxidation of carbon oxide, including preliminary modification of aluminium oxide with nickel oxide in amount (0.03-0.50) % wt, impregnation with acidified with hydrochloric acid solution of palladium (II) chloride, in amount (0.1-1.5) % wt in terms of metal, reduction with sodium formiate solution with rate of solution feeding (0.1-0.4) cm/s with further washing and drying of catalyst first at room temperature during (1-2) h, then at temperature (30-40)°C during (1-2) h and then to temperature (105-115)°C with rate of its increase (10-15)°C/h.

EFFECT: obtaining more efficient catalyst for carbon oxide oxidation in wide range of its concentrations at room temperature of use.

2 tbl, 13 ex

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RU 2 339 446 C1

Authors

Makljaev Vladimir Petrovich

Antonova Natal'Ja Mikhajlovna

Pashchenko Galina Petrovna

Chebykin Valentin Vasil'Evich

Dzisjak Anatolij Petrovich

Glazunova Larisa Dmitrievna

Tikhomirov Evgenij Vladimirovich

Kordialik Vsevolod Vladislavovich

Gartsman Izrail' Iosifovich

Dates

2008-11-27Published

2007-08-03Filed