FIELD: chemistry.
SUBSTANCE: invention refers to method of producing high-quality vanadium pentoxide from hydrated deposited industrial vanadium pentoxide. Method includes as follows. Deposit is filtered, washed with water with following reagent processing by calcium-containing salt solutions to recover it from manganese. Reagent processing is enabled in ratio 3.0-8.5 g Ca2 + per 1 g MnO. Produced is supplied to reagent processing of new portions of hydrated deposited industrial vanadium pentoxide in the same Ca2 + to MnO ratio. As manganese is accumulated in solution, it is regenerated with adding calcium hydroxide suspension, containing CaO, or slaked lime of consumption 1.0-1.45 g CaO per 1 g MnO in stirring. After that manganese concentrate is isolated. Liquid phase is delivered back to reagent processing of new portions of hydrated deposited industrial vanadium pentoxide.
EFFECT: production of the second end product - manganese concentrate, cost saving of production and enhanced ecology.
1 dwg, 4 tbl, 6 ex
Title | Year | Author | Number |
---|---|---|---|
VANADIUM EXTRACTION METHOD | 1999 |
|
RU2162113C1 |
VANADIUM RECOVERY PROCESS | 2000 |
|
RU2169203C1 |
METHOD OF PROCESSING OF VANADIUM-CONTAINING CONVERTER SLAGS | 1999 |
|
RU2157420C1 |
METHOD OF OBTAINING VANADIUM PETROXIDE OF HIGH-PURITY | 1983 |
|
SU1208818A1 |
METHOD FOR VANADIUM RECOVERY | 2003 |
|
RU2245936C1 |
METHOD OF PROCESSING VANADIUM-CONTAINING CONVERTER SLAG | 2003 |
|
RU2266343C2 |
PROCESS FOR RECOVERY OF VANADIUM FROM SULFATE SOLUTIONS | 1995 |
|
RU2085603C1 |
METHOD OF PROCESSING VANADIUM CONTAINING CONVERTER SLAG | 2008 |
|
RU2385353C2 |
METHOD OF PREPARING VANADIUM COMPOUNDS | 1998 |
|
RU2124479C1 |
METHOD OF OBTAINING VANADIUM PENTOXIDE | 1993 |
|
RU2044785C1 |
Authors
Dates
2009-04-10—Published
2007-09-26—Filed