METHOD OF BIRCH BARK PROCESSING Russian patent published in 2009 - IPC A61K36/00 C08H5/04 C07J9/00 

Abstract RU 2359688 C1

FIELD: production processes.

SUBSTANCE: invention refers to wood working and wood chemical industries. Birch bark is broken down, mixed with liquid, the mixture is held at temperature higher than mixture freezing temperature, then triterpene compounds are separated from lingo-adipic residue with the following filtration and drying. Birch bark is additionally broken down by method of impact-abrasing and/or abrasing effect till obtaining birch bark flour. Birch bark flour is mixed with liquid with density of 0.999-0.958 kg/m3. Mixture is held for 0.1-10 hours and then separated by flotation to hydrophobic and hydrophilous fraction. Solution remaining after separation is condensed and dried. Obtained hydrophobic fraction - mixture of triterpene compounds - is exposed to recrystallisation in ethanol with activated charcoal and then betuline, solution of triterpene compounds in ethanol and mixture of triterpene and polyphenol compounds at carbon matrix is obtained. Or triterpene compounds mixture is separated to fractions in carbon-dioxide extractor and betuline, dry mixture of triterpene and polyphenol compounds are obtained. Hydrophilous fraction - lingo-adipic flour - is separated from liquid and dried out.

EFFECT: increase of environmental safety and method effectiveness.

6 cl, 4 ex, 3 dwg

Similar patents RU2359688C1

Title Year Author Number
BIRCH BARK PROCESSING METHOD 2006
  • Sirotkin Gennadij Vladimirovich
  • Miftakhov Aleksandr Rashitovich
  • Kul'Gashov Jurij Aleksandrovich
  • Makhova Nadezhda Nikolaevna
  • Tolina Marija Valentinovna
RU2305550C1
METHOD OF BETULINOL PREPARING 2000
  • Sirotkin G.V.
  • Sternin Ju.I.
RU2172178C1
METHOD FOR COMPLEX PROCESSING OF BIRCH BARK 2016
  • Kuznetsov Boris Nikolaevich
  • Sudakova Irina Gennadevna
  • Kuznetsova Svetlana Alekseevna
  • Grishechko Lyudmila Ivanovna
  • Skvortsova Galina Pavlovna
  • Veprikova Evgeniya Vladimirovna
  • Levdanskij Vladimir Aleksandrovich
RU2618892C1
METHOD OF OBTAINING BETULIN (VERSIONS) 2013
  • Klimakov Vladimir Sergeevich
  • Zorin Aleksandr Vladimirovich
  • Vershinin Stanislav Stanislavovich
  • Zorin Vladimir Viktorovich
RU2523545C1
METHOD OF ISOLATION OF BETULINOL 2002
  • Borts M.S.
  • Nikolaeva E.G.
  • Laevskij I.S.
RU2206572C1
WAY OF RECEPTION OF BIOLOGICALLY ACTIVE SUBSTANCES FROM BIRCH BARK 2008
  • Levdanskij Vladimir Aleksandrovich
  • Levdanskij Aleksandr Vladimirovich
  • Kuznetsov Boris Nikolaevich
RU2363486C1
METHOD OF BIRCH BARK CONVERSION 2008
  • Levdanskij Vladimir Aleksandrovich
  • Levdanskij Aleksandr Vladimirovich
  • Kuznetsov Boris Nikolaevich
RU2352350C1
METHOD OF BIRCH BARK CONVERSION 2008
  • Levdanskij Vladimir Aleksandrovich
  • Levdanskij Aleksandr Vladimirovich
  • Kuznetsov Boris Nikolaevich
RU2352349C1
CARRIER FOR MEDICINAL AND DIAGNOSTIC AGENTS 2006
  • Kaplun Aleksandr Petrovich
  • Illarionov Vladimir Vladimirovich
  • Balakshin Vladimir Vladimirovich
  • Chistjakov Aleksej Nikolaevich
RU2322998C1
METHOD OF PRODUCING BETULIN 2017
  • Ivakhnov Artem Dmitrievich
  • Skrebets Tatyana Eduardovna
  • Kosyakov Dmitrij Sergeevich
  • Ulyanovskij Nikolaj Valerevich
  • Kozhevnikov Aleksandr Yurevich
RU2668976C1

RU 2 359 688 C1

Authors

Kiselev Oleg Ivanovich

Sirotkin Gennadij Vladimirovich

Kul'Gashov Jurij Aleksandrovich

Miftakhov Aleksandr Rashitovich

Efimova Ljubov' Vladimirovna

Makhova Nadezhda Nikolaevna

Tolina Marija Valentinovna

Dates

2009-06-27Published

2008-01-09Filed