METHOD OF OBTAINING POLYMETHYLMETHACRYLATE Russian patent published in 2010 - IPC C08F120/14 B01J31/22 

Abstract RU 2394045 C2

FIELD: chemistry.

SUBSTANCE: described is a method of obtaining polymethylmethacrylate via radical polymerisation in a methylmethacrylate mass in the presence of an initiating system, one of the components of which is benzoyl peroxide. The method is distinguished by that, the second component of the initiating system used is bis-ferrocenylborate macrobicyclic tris-1,2-cyclohexanedionedioxymate of iron (II), molar ratio bis-ferrocenylborate macrobicyclic tris-1,2-cyclohexanedionedioxymate of iron (II): benzoyl peroxide equals (0.01-0.1):(0.05-1) and polymerisation is carried out at 30-60°C.

EFFECT: faster polymerisation, reduced consumption of components of the initiating system, lower polymerisation temperature, elimination of the gel effect, regulation of molecular weight of the obtained polymethylmethacrylate.

1 cl, 1 tbl, 5 ex

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RU 2 394 045 C2

Authors

Monakov Jurij Borisovich

Islamova Regina Maratovna

Sadykova Guzel' Rifatovna

Voloshin Jan Zigfridovich

Makarov Il'Ja Stanislavovich

Bubnov Jurij Nikolaevich

Dates

2010-07-10Published

2008-08-04Filed