CAMPHOLENE ALDEHYDE SYNTHESIS METHOD Russian patent published in 2010 - IPC C07C47/225 C07C45/67 

Abstract RU 2402522 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method for synthesis of campholene aldehyde which is widely used in perfumery and household chemicals. The method involves conversion of α-pinene epoxide in a supercritical complex solvent consisting of a mixture of carbon dioxide, propanol-2 and water at temperature of 160-240°C and pressure of 130-220 atm. As a rule, the conversion reaction is carried out in a supercritical solvent with molar ratio water/α-pinene epoxide equal to 5-7.9.

EFFECT: method increases rate and efficiency of the chemical process to obtain an end product with high output and with controlled selectivity.

2 cl, 1 tbl, 6 ex

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Authors

Anikeev Vladimir Il'Ich

Il'Ina Irina Viktorovna

Volcho Konstantin Petrovich

Salakhutdinov Nariman Faridovich

Dates

2010-10-27Published

2009-05-04Filed