FIELD: metallurgy.
SUBSTANCE: tetrakis-(tri-fluoro-phosphide) of palladium is synthesised out of palladium chloride and phosphorus fluoride (III) at pressure of phosphorus fluoride (III) as high, as 26 at and temperature as high, as 120°C. Condensation of synthesised tetrakis-(tri-fluoro-phosphide) of palladium is performed at temperature as low as -50°C.
EFFECT: reduced operational expenditures, increased service life of equipment, raised safety and efficiency of process.
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