FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing porous bioactive glass-ceramic material. Said method involves preparing a semidry mass containing powdered calcium phosphate glass and 1-10% solution of a polymer selected from polyvinyl alcohol, gelatine, methyl cellulose or carboxymethyl cellulose, which is then moulded in paper masters at moulding pressure 1.0-1.2 MPa, dried, burnt and held for 0.5-1.5 hours at 900-1000°C. Main channel foaming agents in form of caprone, nylon, lavsan or graphite in amount of 3-30 wt % and starch in amount of 1-10 wt % are then added to the semidry mass. The calcium phosphate glass has the following composition in mol %: CaO - 40-55, Al2O3 - 4-10, B2O3 - 1-5, TiO2 - 1-10, ZrO2 - 1-10 and P2O5 - the balance.
EFFECT: method enables to obtain bioactive glass-ceramic materials for implantation with a channel and an inter-channel pore structure with open porosity of 20-70%, content of pore channels of 5-40%, channel pore diameter of 100-700 mcm, pore size in inter-channel partitions of 20-100 mcm.
2 cl, 8 ex
Title | Year | Author | Number |
---|---|---|---|
ZIRCONIUM OXIDE-BASED METHOD FOR PRODUCING POROUS BIOACTIVE CERAMICS | 2015 |
|
RU2595703C1 |
METHOD FOR PRODUCING BIOGLASS DOPED WITH ZIRCONIUM DIOXIDE | 2021 |
|
RU2765471C1 |
METHOD FOR PRODUCING BIOACTIVE CERAMICS BASED ON ZIRCONIUM DIOXIDE | 2021 |
|
RU2771017C1 |
BIOACTIVE MICROCELLULAR MATERIAL FOR ORTHOPAEDIC SURGERY AND METHOD FOR MAKING IT | 2010 |
|
RU2452515C1 |
COMPOSITE BASED ON ALUMINOSILICATE GLASS CERAMICS AND METHOD OF OBTAINING THEREOF (VERSIONS) | 2013 |
|
RU2534229C2 |
METHOD OF HIGH-POROUS MATERIAL RECEIVING | 2007 |
|
RU2353474C2 |
LOW-MELTING GLASS COMPOSITION | 2018 |
|
RU2697352C1 |
PROCEDURE FOR PRODUCTION OF HIGH POROUS MATERIAL | 2008 |
|
RU2408741C2 |
METHOD FOR PRODUCTION OF HIGHLY POROUS CELLULAR GLASS-CERAMIC MATERIAL | 2007 |
|
RU2352544C1 |
METHOD FOR PRODUCTION OF HIGHLY POROUS CELLULAR STRUCTURE FROM CERAMICS | 2007 |
|
RU2348487C2 |
Authors
Dates
2012-09-27—Published
2010-06-23—Filed