METHOD OF PURIFYING BETULIN Russian patent published in 2012 - IPC C07J53/00 C07J63/00 

Abstract RU 2463306 C1

FIELD: chemistry.

SUBSTANCE: extract of plant material containing betulin is dissolved in a hydrocarbon solvent or mixtures thereof with boiling point in the range of 120…250°C, heated to boiling and boiled while stirring until complete dissolution of betulin. The insoluble fraction of polyolefins and phytosterols is separated by hot filtration of the obtained solution and dried in a vacuum at temperature 80°C. The filtrate is then cooled to temperature 0…5°C, wherein the precipitated betulin is filtered and also dried in a vacuum at temperature 80°C. Also, the mixture of hydrocarbons of the solvent can contain up to 20% aromatic hydrocarbons.

EFFECT: method achieves more complete extraction and separation of products of processing plant maerial.

2 cl, 2 ex, 1 tbl

Similar patents RU2463306C1

Title Year Author Number
METHOD OF PREPARING EXTRACTIVE SUBSTANCES FROM BIRCH BARK 2006
  • Zhuk Vladislav Vital'Evich
  • Bakibaev Abdigali Abdimanapovich
  • Medvedev Dmitrij Mikhajlovich
  • Janovskij Vjacheslav Aleksandrovich
  • Jagovkin Aleksandr Jur'Evich
RU2298558C1
METHOD OF OBTAINING BETULIN BISFORMATE 2018
  • Arrus Salakh
  • Bakibaev Abdigali Abdimanapovich
  • Malkov Viktor Sergeevich
RU2678819C1
METHOD FOR PREPARING DIPHENIC ACID N-SUBSTITUTED IMIDES 2005
  • Janovskij Vjacheslav Aleksandrovich
  • Shardakov Oleg Nikolaevich
  • Jagovkin Aleksandr Jur'Evich
  • Bakibaev Abdigali Abdimanapovich
RU2285694C1
METHOD FOR COMPLEX PROCESSING OF BIRCH BARK 2016
  • Kuznetsov Boris Nikolaevich
  • Sudakova Irina Gennadevna
  • Kuznetsova Svetlana Alekseevna
  • Grishechko Lyudmila Ivanovna
  • Skvortsova Galina Pavlovna
  • Veprikova Evgeniya Vladimirovna
  • Levdanskij Vladimir Aleksandrovich
RU2618892C1
METHOD OF PROCESSING PLANT RAW MATERIALS 2023
  • Shamsullin Airat Insafovich
  • Shigapov Niiaz Marsovich
  • Zaikin Pavel Anatolevich
  • Saiko Anastasiia Vasilevna
  • Minnibaev Aidar Samigullovich
RU2812565C1
METHOD FOR ISOLATING NEUTRAL SUBSTANCES FROM HARDWOOD SULPHATE SOAP 2023
  • Vedernikov Dmitrij Nikolaevich
  • Shelomentsev Vladislav Valerevich
  • Ulyanova Ekaterina Alekseevna
RU2814488C1
METHOD OF CHEMICALLY PROCESSING BIRCH BARK 2005
  • Kislitsyn Aleksej Nikolaevich
  • Klabukova Irina Nikolaevna
  • Trofimov Anatolij Nikiforovich
RU2306318C2
METHOD OF PRODUCING BETULIN 2013
  • Mal'Chikov Evgenij Leonidovich
  • Kislitsyn Aleksej Nikolaevich
RU2524778C1
METHOD OF PROCESSING VEGETABLE MATTER 2003
  • Roshchin V.I.
  • Sultanov V.S.
RU2238291C1
METHOD FOR THE ISOLATION OF PHYTOSTEROLS FROM TALL PITCH 2017
  • Chernov Ilya Nikolaevich
  • Korshunov Aleksej Olegovich
  • Dolinskij Taras Ivanovich
  • Lazarev Mikhail Alekseevich
  • Mavrina Ekaterina Aleksandrovna
  • Ilichev Ilya Sergeevich
  • Radbil Arkadij Benyuminovich
RU2655444C1

RU 2 463 306 C1

Authors

Janovskij Vjacheslav Aleksandrovich

Andrienko Oleg Semenovich

Zhuk Vladislav Vital'Evich

Bakibaev Abdigali Abdimanapovich

Sachkov Viktor Ivanovich

Dates

2012-10-10Published

2011-07-28Filed