METHOD OF MAKING ALUMINIUM OXIDE-BASED MEMBRANES Russian patent published in 2013 - IPC B01D67/00 B82B3/00 

Abstract RU 2474466 C1

FIELD: process engineering.

SUBSTANCE: invention relates to production of membranes and may be used in nanotechnologies for making various filters, templates for making membrane nanocatalysts, production of capillary pumps, etc. proposed method is implemented as follows. Processed aluminium specimen is subjected to primary anodising at 20-60 V, current density of 100-500 mA/cm2, temperature of 20-25°C for 5-10 min. Formed poorly ordered aluminium oxide layer is removed by applying short cathode voltage pulse of +(20-60) V to -(20-60)V and duration of at least 10 s. Thereafter, secondary anodising is carried out to make porous ordered-structure oxide layer of aluminium. Removing barrier layer, exposing pore bottom and separating formed ordered-structure membrane is carried out by applying short cathode voltage pulse of +(40-60) V to -(40-60)V and duration of at least 5-20 s.

EFFECT: simplified process, lower costs, decreased process cycle.

3 cl, 10 dwg, 3 ex

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RU 2 474 466 C1

Authors

Kondrikov Nikolaj Borisovich

Tsarev Sergej Aleksandrovich

Dates

2013-02-10Published

2011-08-09Filed