FIELD: chemistry.
SUBSTANCE: method involves soaking starting cellulose fibre with an aqueous solution containing 6.5% dibasic ammonium phosphate, 10.6% ammonium chloride and 2.5% sodium chloride at 30°C for 30 minutes, followed by pressing. The fibre is then dried at 95±5°C using a microwave source and then heat treated in a medium of methane to 220°C. The partially carbonised material is heated in a medium of nitrogen to 2400°C. The microwave source has output power of 1-50 kW and operating frequency of 100-300 MHz.
EFFECT: invention increases efficiency of the method of producing carbon fibre with high strength.
2 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF CARBON FIBROUS MATERIAL PREPARING | 1991 |
|
RU2016146C1 |
METHOD OF PRODUCING CARBON FIBRE MATERIALS | 2015 |
|
RU2596752C1 |
APPARATUS FOR PRODUCING CARBON FIBER MATERIALS | 2015 |
|
RU2645208C2 |
METHOD OF MAKING BILLETS FROM FINE-GRAINED GRAPHITE | 2011 |
|
RU2488554C2 |
METHOD FOR PRODUCING CARBON NON-WOVEN FIBROUS FABRIC FROM HYDRATED CELLULOSE FIBERS | 2022 |
|
RU2797209C1 |
METHOD OF PRODUCING CARBON FIBROUS MATERIALS FROM HYDRATE-AND-CELLULOSE FIBERS | 2020 |
|
RU2740139C1 |
METHOD OF PRODUCING CARBON FIBRE MATERIALS FROM VISCOSE FIBRES | 2012 |
|
RU2502836C2 |
METHOD OF TREATING PARTIALLY CARBONIZED CARBON FIBROUS MATERIAL PRIOR TO GRAPHITIZATION | 2018 |
|
RU2708208C1 |
METHOD OF PRODUCING CARBON NONWOVEN FIBROUS MATERIAL | 2017 |
|
RU2670884C1 |
PROCEDURE FOR CONTINUOUS PRODUCTION OF HYDRATED CELLULOSE OF CARBON FIBRE IN FORM OF UNIDIRECTIONAL BRAID | 2010 |
|
RU2429316C1 |
Authors
Dates
2013-02-20—Published
2011-10-21—Filed