FIELD: chemistry.
SUBSTANCE: invention relates to a method of producing curing agents of epoxy resins involving an operation for reacting amines with monocarboxylic acids. The method is characterised by that the amine component used is a mixture consisting of a primary aromatic amine or a mixture of aromatic amines (A), a secondary aliphatic amino alcohol (B) and a tertiary aliphatic amino alcohol (C) in weight ratio A:B:C from 98:0.2:1.8 to 80:5:15. The monocarboxylic acid (D) is used in form of a 25-80% solution in a monoatomic aliphatic or aromatic alcohol, or ester thereof with a mono- or dicarboxylic acid, in ratio (A+B+C):D from 90:10 to 60:40 per 100% acid. The reaction process is then carried out by mixing in a reactor at temperature ranging from 50 to 130°C for 20 to 120 minutes and speed of the mixer of 100 to 3000 rpm.
EFFECT: curing agents obtained using said method have high stability during storage.
1 cl, 7 ex, 1 tbl
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Authors
Dates
2013-02-27—Published
2011-12-28—Filed