METHOD OF PRODUCING CATALYST FOR HYDROFINING DIESEL FUEL Russian patent published in 2013 - IPC B01J37/04 B01J23/88 B01J23/755 B01J37/34 C10G45/08 B01J21/02 

Abstract RU 2491123 C1

FIELD: chemistry.

SUBSTANCE: invention relates to catalytic chemistry, particularly a method of producing aluminium-nickel-molybdenum catalysts for hydrofining diesel fuel by self-propagating high-temperature synthesis through an intermetallic alloy step. The method of producing the catalyst involves mixing dry powder of nickel, molybdenum and aluminium oxides in ratio of 35-67% molybdenum oxide, 9-17% nickel oxide, aluminium oxide - the balance; the obtained mixture is used to mould pellets of given size and mass, which are then placed into a refractory mould with an inner high-temperature protective coating; said mould is placed a centrifuge and then rotated with centrifugal acceleration of 4-80 g, where g gravitational acceleration; during rotation of the centrifuge, the pellets are burnt and the combustion process is maintained in an air atmosphere at temperature higher than the melting point of components of the mixture of the pellets until an intermetallic alloy is obtained; after removing from the centrifuge, the obtained alloy is then successively leached from aluminium with an alkali metal hydroxide solution for 20-60 minutes, washed and stabilised with 10% citric acid solution and 1% hydrogen peroxide solution.

EFFECT: fewer steps of preparing the catalyst and obtaining a highly active catalyst.

4 tbl, 4 ex

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RU 2 491 123 C1

Authors

Borshch Vjacheslav Nikolaevich

Sanin Vladimir Nikolaevich

Jukhvid Vladimir Isaakovich

Kolesnikov Sergej Ivanovich

Chekhovskaja Ol'Ga Mansurovna

Jablonskij Aleksandr Vjacheslavovich

Kil'Janov Mikhail Jur'Evich

Sysoev Vladimir Anatol'Evich

Vinokurov Vladimir Arnol'Dovich

Ivanov Evgenij Vladimirovich

Gushchin Pavel Aleksandrovich

Kolesnikov Ivan Mikhajlovich

Dates

2013-08-27Published

2012-07-17Filed