FIELD: chemistry.
SUBSTANCE: claimed is method of triphenylene synthesis by successive interaction of cyclohexanone with NaOH, polyphosphoric acid at first stage with obtaining dodecahydrotriphenylene, which is processed with catalyst in argon atmosphere at second stage. Continuous extraction with release of dodecahydrotriphenylene is applied at first stage. Palladium on sibunit catalyst is applied at second stage. In the course of reaction with catalyst highly pure triphenylene is sublimated onto cold surface. 
EFFECT: method of synthesis makes it possible to obtain highly pure sublimated triphenylene with good output from available reagents.
1 ex
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD FOR SYNTHESIS OF 2,3,6,7,10,11-TRIS-(9H,10H-ANTHRACENE-9,10-DIIYL)TRIPHENYLENE - MONOMOLECULAR OPTICAL SENSOR FOR DETECTING NITROAROMATIC COMPOUNDS | 2012 |
|
RU2485084C1 |
| METHOD OF PRODUCING 1,4-DISUBSTITUTED [1.1.1.1.1] PENTIPTICENES | 2011 |
|
RU2474568C1 |
| METHOD OF OBTAINING BRANCHED OLIGOARYLSYLANES BASED ON PHENYLOXAZOLS | 2016 |
|
RU2620088C1 |
| METHOD FOR OBTAINING 1-PHENYL-1-BORASPYROALKANE | 2022 |
|
RU2800048C1 |
| METHOD FOR OBTAINING 4,4'-BINAPHTHYL-1,1',8,8'-TETRACARBOXYLIC ACID FROM HALOGENACENAPHTHENES | 2017 |
|
RU2671579C1 |
| METHOD OF OBTAINING DIANHYDRIDES OF AROMATIC TETRACARBONIC ACIDS | 2017 |
|
RU2682170C1 |
| SYNTHESIS OF BUILDING BLOCKS AND STARTING SUBSTANCES FOR OBTAINING RENEWABLE POLYMERS | 2018 |
|
RU2799800C2 |
| METHOD FOR OBTAINING PALLADIUM ANILINE COMPLEXES | 2015 |
|
RU2618526C1 |
| METHOD OF PRODUCING 4'-(TRIFLUOROMETHYL)-2,2':6',2''-TERPYRIDINE | 2020 |
|
RU2723682C1 |
| METHOD OF OBTAINING N,N'-BIS-(3-MERCAPTOPHENYL)TETRATHIADIAZACYCLOALKANES | 2013 |
|
RU2538595C1 |
