METHOD OF PRODUCING 4-[(3-ETHOXY-3-OXOPROPANOYL)AMINO]BENZOIC ACID Russian patent published in 2014 - IPC C07C231/02 C07C235/80 

Abstract RU 2515245 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 4-[(3-ethoxy-3-oxopropanoyl)amino]benzoic acid. The method involves reacting diethyl ether of malonic acid with 4-aminobenzoic acid while heating in the presence of an organic solvent. The organic solvent used is an aromatic solvent selected from toluene or o-xylene; the process is carried out at boiling point of the reaction mass (120-150°C) for 2-5 hours with molar ratio of 4-aminobenzoic acid and ethyl ether of malonic acid of 1:4, followed by separation of the end product.

EFFECT: method cuts the duration of the process, lowers the temperature thereof and increases the output of the end product.

3 cl, 2 ex

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RU 2 515 245 C1

Authors

Juskovets Valerij Nikolaevich

Jakovlev Igor' Pavlovich

Narkevich Igor' Anatol'Evich

Dates

2014-05-10Published

2013-02-07Filed