METHOD OF DETERMINING THIACLOPRID IN BIOLOGICAL OBJECTS USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY Russian patent published in 2014 - IPC G01N30/95 

Abstract RU 2517075 C1

FIELD: veterinary medicine.

SUBSTANCE: method comprises sampling, extraction, filtration, dehydration of sodium with anhydrous sulphate, vaporisation, introduction of the dissolved dry residue in the liquid chromatograph, processing the results of the analysis, a weigh of organs or tissues from animals weighing 50 to 200 mg is taken as the sample, extraction is performed with acetone, the dissolved dry residue is put to the liquid chromatograph "Chromos-ZhH301" with the spectrophotometric detector UVV 104M, a column Diasfer-NOS-16 (150×4) mm is used with a pore size of sorbent of 5 microns, a mixture of acetonitrile and water in a ratio of 30:70 is used as eluent.

EFFECT: increased sensitivity and selectivity of the analysis.

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Authors

Bojko Tat'Jana Vladimirovna

Gerunova Ljudmila Karpovna

Gonokhova Marina Nikolaevna

Luksha Elena Aleksandrovna

Urusova Tat'Jana Vladimirovna

Temerova Elena Valentinovna

Goncharov Dmitrij Sergeevich

Pogodin Il'Ja Sergeevich

Dates

2014-05-27Published

2012-10-09Filed