METHOD FOR DETERMINATION OF PESTICIDES IN BIOLOGICAL MATERIAL USING HPLC Russian patent published in 2016 - IPC G01N33/00 

Abstract RU 2598733 C2

FIELD: ecology.

SUBSTANCE: invention relates to ecology, namely to method for simultaneous determination of pesticides of various chemical classes in biological material. For this purpose, fish liver is homogenised with anhydrous sodium sulphate and sodium hydro citrate, extracted with acetonitrile, shaken and settled. Then sample is centrifuged at 3,000 rpm and sorbents such as silica gel C-18, Bondesil-PSA and anhydrous sodium sulphate are added, then centrifugation is repeated. Obtained solution is evaporated, dry residue is dissolved in acetonitrile and analysed by HPLC with UV detector.

EFFECT: invention allows evaluating of pesticides contamination level in biological objects during environmental monitoring.

1 cl, 2 dwg, 4 ex

Similar patents RU2598733C2

Title Year Author Number
METHOD FOR DETERMINING NEONICOTINOIDS IN A DEAD BEES USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY 2019
  • Sajfutdinov Aleksandr Maratovich
  • Egorov Vladislav Ivanovich
  • Semenov Eduard Ilyasovich
  • Yamalova Guzaliya Rustamovna
  • Abulkhanov Alfred Gilmanovich
  • Burkin Konstantin Evgenevich
  • Galyautdinova Gulnara Gabitovna
  • Khalikova Kadriya Fagimovna
RU2730399C1
METHOD OF DETERMINING 2,4,6-TRINITROMETHYLBENZENE IN BIOLOGICAL MATERIAL 2006
  • Shormanov Vladimir Kambulatovich
  • Omel'Chenko Vladimir Aleksandrovich
RU2319142C1
METHOD OF DETERMINING 2,4-DICHLOROPHENOXY ACETIC ACID IN BIOLOGICAL MATERIAL 2011
  • Shormanov Vladimir Kambulatovich
  • Korolev Vladimir Anatol'Evich
  • Koropova Tat'Jana Fedorovna
  • Altukhova Anna Aleksandrovna
RU2453848C1
METHOD FOR BIOLOGICAL MATERIAL ANALYSIS FOR TETRAMETHYLTHIURAMSULPHIDE 2009
  • Shormanov Vladimir Kambulatovich
  • Korolev Vladimir Anatol'Evich
  • Ivanov Vladimir Petrovich
  • Kim Alla Vital'Evna
  • Duritsyn Evgenij Petrovich
  • Prosvetova Anastasija Petrovna
RU2415425C1
METHOD OF PREPARING BIOLOGICAL SAMPLES FOR DETERMINING POLYCYCLIC AROMATIC HYDROCARBONS 2011
  • Pavlenko Lilija Fedorovna
  • Skrypnik Galina Vasil'Evna
  • Larin Andrej Aleksandrovich
  • Ehkilik Viktorija Sergeevna
RU2461824C1
METHOD FOR DETERMINATION OF O-(2,3-DIHYDRO-2,2-DIMETHYL-7-BENZOFURANYL)-N-METHYLCARBAMATE AND O-(2,3-DIHYDRO-2,2-DIMETHYL-7-BENZOFURANYL)-N-(DIBUTYLAMINOSULPHENYL)-N-METHYLCARBAMATE IN BIOLOGICAL MATERIAL 2016
  • Shormanov Vladimir Kambulatovich
  • Galushkin Svyatoslav Gennadevich
  • Kovalenko Evgenij Anatolevich
RU2623070C1
METHOD FOR DETERMINATION OF 2-DIMETHYLAMINO-1,3-BIS-(PHENYLSULFONYLTHIO)PROPANE IN BIOLOGICAL MATERIAL 2017
  • Shormanov Vladimir Kambulatovich
  • Baranov Yurij Nikolaevich
  • Kovalenko Evgenij Anatolevich
RU2647477C1
METHOD FOR DETERMINATION OF O-(2,3-DIHYDRO-2,2-DIMETHYL-7-BENZOFURANYL)-N-METHYLCARBAMATE IN BIOLOGICAL SAMPLE 2004
  • Shormanov Vladimir Kambulatovich
  • Kovalenko Evgenij Anatol'Evich
  • Ivanov Vladimir Petrovich
  • Korolev Vladimir Anatol'Evich
  • Duritsyn Evgenij Petrovich
  • Pistunovich Elena Vladimirovna
RU2269780C1
METHOD OF DETERMINING MYCOTOXINS IN ANIMAL AND VEGETABLE PRODUCTS 2012
  • Amelin Vasilij Grigor'Evich
  • Tret'Jakov Aleksej Viktorovich
  • Karaseva Nadezhda Mikhajlovna
  • Nikeshina Tat'Jana Borisovna
  • Abramenkova Ol'Ga Igorevna
RU2514828C2
METHOD FOR DETERMINATION OF RESIDUAL AMOUNTS OF FENOXYCARB IN SOIL BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY 2020
  • Podgornaya Marina Efimovna
  • Didenko Nadezhda Aleksandrovna
RU2760530C1

RU 2 598 733 C2

Authors

Zinchuk Olga Anatolevna

Valiullin Vasil Akramovich

Bugaev Leonid Anatolevich

Vojkina Anna Vladimirovna

Karpushina Yuliya Eduardovna

Dates

2016-09-27Published

2014-12-31Filed