FIELD: chemical analysis.
SUBSTANCE: invention relates to a method for determining the residual amounts of fenoxycarb in the soil by high-performance liquid chromatography, including sample preparation: extraction from the soil, subsequent purification of the extract in a system of immiscible solvents: hexane, saturated sodium chloride solution, aqueous sodium bicarbonate solution and directly quantitative determination of fenoxycarb in the soil by high-performance liquid chromatography, and at the extraction stage the less toxic carbon tetrachloride is used as a solvent, and at the stage of purification of the extract, a corrugated filter was used.
EFFECT: extension of the range of methods for determining chemical substances in soil.
1 cl, 2 ex, 3 tbl, 4 dwg
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR DETERMINING NEONICOTINOIDS IN A DEAD BEES USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY | 2019 |
|
RU2730399C1 |
METHOD FOR DETERMINATION OF CHLORAMPHENICOL CONTENT IN FOOD PRODUCTS AND SORBENT FOR ITS IMPLEMENTATION | 2010 |
|
RU2431829C1 |
METHOD OF QUANTITATIVE DETERMINATION OF HEXACHLOROBENZENE IN BLOOD BY METHOD OF GAS CHROMATOGRAPHIC ANALYSIS | 2016 |
|
RU2613306C1 |
METHOD OF DETERMINING IMIDACLOPRID IN BIOLOGICAL OBJECTS USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY | 2011 |
|
RU2484458C1 |
METHOD FOR DETERMINING CONTENT OF FUMARIC AND MALEIC ACIDS IN BLOOD PLASMA BY METHOD OF HIGHLY EFFECTIVE LIQUID CHROMATOGRAPHY | 2018 |
|
RU2677341C1 |
METHOD FOR DETERMINATION OF DEPRESSANT-DISPERSANT ADDITIVES IN DIESEL FUEL | 2021 |
|
RU2756706C1 |
METHOD FOR DETERMINATION OF MASS CONCENTRATIONS OF PHENOL AND PYROCATECHOL IN BLOOD BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY | 2022 |
|
RU2786509C1 |
METHOD OF EXTRACTING 3,4-BENZ(A)PYRENE FROM SOIL, BOTTOM DEPOSITS AND WASTE WATER SLUDGE | 2012 |
|
RU2485109C1 |
METHOD FOR PREPARING SAMPLE FOR QUANTITATIVE DETERMINATION OF CONTENT OF FAT-SOLUBLE VITAMIN IN ANALYZED SAMPLE BY HPLC METHOD | 2023 |
|
RU2824398C1 |
METHOD OF DETERMINING THIACLOPRID IN BIOLOGICAL OBJECTS USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY | 2012 |
|
RU2517075C1 |
Authors
Dates
2021-11-26—Published
2020-10-20—Filed