FIELD: chemistry.
SUBSTANCE: as initial reagent used is 2-chloro-5-hydroxymethylpyridine, and as chlorinating agent - cyanuric chloride, which makes it possible to realise reaction of interaction within 90 minutes in standard conditions and obtain 2-chloro-5-chloromethylpyridine with output not less than 90%. 2-chloro-5-chloromethylpyridine is applied in production of neonicotinoids, in particular imidacloprid, thiacloprid, nitenpyram, widely used in agriculture for fighting pests of grain, fruit and vegetable cultures, in household for elimination of insects in residential and industrial premises.
EFFECT: method improvement.
1 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF OBTAINING 2-CHLORO-5-HYDROXYMETHYLPYRIDINE | 2013 |
|
RU2537848C1 |
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RU2539658C1 |
METHOD FOR PREPARING HETEROCYCLIC COMPOUNDS | 2001 |
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RU2269526C2 |
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RU2324698C1 |
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RU2480000C2 |
METHOD OF PRODUCING TERPENE α-CHLOROKETONES OR CHLOROHYDROXYKETONES | 2015 |
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RU2569896C1 |
METHOD FOR PREPARING 3-DICHLOROMETHYLPYRIDINE | 2006 |
|
RU2316547C1 |
DERIVATIVES OF PIPERAZINE | 1998 |
|
RU2197488C2 |
METHOD OF PREPARING CHLORODESOXYCELLULOSE | 0 |
|
SU833983A1 |
IMPROVED METHOD OF PREPARING 2,4-DIAMINO-6-ALKYLTHIO-S-IRIAZINES | 1994 |
|
RU2162080C2 |
Authors
Dates
2015-01-10—Published
2013-12-10—Filed