METHOD OF OBTAINING SOLUTION OF GADOLINIUM DIALKYLPHOSPHATE - COMPONENT OF CATALYSTS OF (CO) Russian patent published in 2015 - IPC C07F5/00 C07F9/09 

Abstract RU 2540083 C1

FIELD: chemistry.

SUBSTANCE: invention relates to method of obtaining solution of gadolinium dialkylphosphate, which can be used in production of synthetic rubbers, cis-1,4-homopolymers and cis-1,4-copolymers of isoprene and butadiene. Claimed method consists in the following: first, mixed are: aliphatic and aromatic solvents with weight ratio 1:(4-5), dialkylphosphoric acid, activator in form of 20-40 wt % solution in water, and polyatomic alcohol, then, intensive mixing is switched on and gadolinium oxide is gradually added. After that mixture is heated to 80-90°C for 10-30 minutes.

EFFECT: method is simple in technological aspect, makes it possible to considerably reduce synthesis time with obtaining solutions of gadolinium dialkylphosphates with low viscosity.

3 cl, 8 ex

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Authors

Bodrova Vera Sergeevna

Bubnova Svetlana Vasil'Evna

Vasil'Ev Valentin Aleksandrovich

Drozdov Boris Trofimovich

Levkovskaja Ekaterina Igorevna

Passova Svetlana Solomonovna

Dates

2015-01-27Published

2013-11-13Filed