METHOD OF PRODUCING HALOGEN-SUBSTITUTED AROMATIC AMINES Russian patent published in 2014 - IPC C07C209/36 C07C211/52 

Abstract RU 2531919 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a novel method of producing halogen-substituted aromatic amines. The method includes hydrogenating halogen-substituted aromatic nitro-compounds in an isopropanol medium in the presence of aluminium oxide as a heterogeneous catalyst. The process is carried out by adding supercritical isopropyl alcohol at temperature of 250-340°C and pressure of 150-220 atm.

EFFECT: conducting the process in said conditions considerably shortens reaction time (less than 6 minutes instead of 3,5-6 hours), does not require use of expensive catalysts and enables to obtain products with high selectivity, output and conversion.

2 cl, 5 tbl, 4 ex

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RU 2 531 919 C1

Authors

Anikeev Vladimir Il'Ich

Sivtsev Vladislav Petrovich

Volcho Konstantin Petrovich

Salakhutdinov Nariman Faridovich

Dates

2014-10-27Published

2013-07-16Filed