FIELD: chemistry.
SUBSTANCE: invention relates to a method of obtaining low-viscous white oils, in which vacuum gasoil is subjected to hydrocracking with the volume ratio of hydrogen to a raw material of 800-1000 nm3/m3, volume rate of the raw material supply of 0.4-0.6 h-1, temperature of 340-360°C and partial pressure of hydrogen of 20-30 MPa on Ni/Mo catalyst, applied on a silica-alumina carrier, with the content of active components counted per the catalyst burnt at a temperature of 600°C, wt %: MoO3 - 35.0, NiO - 15.0, SiO2 - 7.0 or on Ni/W catalyst, applied on the silica-alumina carrier, with the content of active components counter per the catalyst burnt at a temperature of 600°C, wt %: WO3 - 25.0, NiO - 10.0, SiO2 - 5.0. The target fraction with the boiling out temperature from 280 to 340°C, the content of aromatic hydrocarbons above the required norm and the temperature of solidification not higher than minus 10°C is separated from the obtained stream, boiling out in the range of temperatures from 280 to 400°C. Hydration of the target fraction is carried out by its contact with hydrogen with the volume ratio of hydrogen to the raw material of 800-950 nm3/m3 on the catalyst at a temperature of 240-320°C, partial pressure of hydrogen of 6.0-8.0 MPa, volume rate of the raw material supply 0.25-0.5 h-1.
EFFECT: reduction of the technological process of obtaining white oils for the medical purpose.
4 cl, 1 tbl, 5 ex
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Authors
Dates
2015-05-10—Published
2014-02-18—Filed