FIELD: chemistry.
SUBSTANCE: invention relates to the synthesis of biologically active compounds, specifically to the method of producing 3-[1-(1-adamantyl)ethyl]-1,5,3-dithiazepane, having fungicidal activity against Rhizoctonia solani. The method comprises reacting α-methyl-1-adamantylmethylamine with 1-oxa-3,6-dithiacycloheptane in the presence of a SmCl3·6H2O catalyst with the molar ratio of α-methyl-1-adamantylmethylamine:1-oxa-3,6-dithiacycloheptane:SmCl3·6H2O=1:1:(0.03-0.07) at the temperature of ~20°C and atmospheric pressure for 2.5-3.5 hours. The output of 3-[1-(1-adamantyl)ethyl]-1,5,3-dithiazepane (1) is equal to 64-72%.
EFFECT: high output.
3 cl, 2 tbl, 1 ex
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