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2 584 692

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(51)

IPC

C07D285/36(2006-01-01)

A01P3/00(2006-01-01)

(21) (22)

Application

2014130397/04, 2014-07-22

(24)

Start date

2014-07-22

(22)

Actual filing date

2014-07-22

(45)

Published

2016-05-20

(72)

Inventor

Dzhemilev Usein MemetovichIbragimov Askhat GabdrakhmanovichGalimzjanova Nailja FauatovnaRakhimova Elena BorisovnaIsmagilov Rinat Arfikovich

(73)

Holder

Federalnoe Gosudarstvennoe Bjudzhetnoe Uchrezhdenie Nauki Institut Neftekhimii I Kataliza Rossijskoj Akademii Nauk

METHOD OF PRODUCING 3-(1-ADAMANTYL)-1,5,3-DITIAZEPANE AND USE THEREOF AS FUNGICIDALLY ACTIVE AGENT Russian patent published in 2016 - IPC C07D285/36 A01P3/00

Abstract RU 2584692 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing 3-(1-adamantyl)-1,5,3-ditiazepane of formula (1) Method involves in reaction of 1-aminoadamantane with 1-oxa-3,6-ditiacycloheptane in presence of catalyst SmCl₃·6H₂O in molar ratio of 1-aminoadamantae:1-oxa-3,6-ditiacyclogeptane:SmCl₃·6H₂O=1:1:(0.03-0.07) at temperature of ~20 °C and atmospheric pressure for 2.5-3.5 hours. Output of 3-(1-adamantyl)-1,5,3-ditiazepane (1) is equal to 69-77 %.

EFFECT: obtained compound has fungicidal activity against Rhizoctonia solani.

3 cl, 2 tbl, 1 ex

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RU 2 584 692 C2

Authors

Dzhemilev Usein Memetovich

Ibragimov Askhat Gabdrakhmanovich

Galimzjanova Nailja Fauatovna

Rakhimova Elena Borisovna

Ismagilov Rinat Arfikovich

Dates

2016-05-20—Published

2014-07-22—Filed