ELECTROCHEMICAL METHOD FOR PRODUCING NANO-SIZED TITANIUM (IV) OXIDE STRUCTURES Russian patent published in 2016 - IPC C01G23/47 C25B1/00 B82B3/00 B82Y40/00 

Abstract RU 2602126 C2

FIELD: chemistry.

SUBSTANCE: invention can be used in producing heterogeneous catalysts with highly developed surface, and electrodes in lithium-ion batteries. Electrochemical method for producing nano-sized titanium (IV) oxide structures involves anodic oxidation of titanium electrode in ionic liquid with addition of water or propylene glycol in an air atmosphere. Ionic liquid has general formula K+A-, where K+ - alkylimideazoline, A- -NTf2-, or PF6-, or Cl-. Anodic oxidation is carried out at 20-25 °C for 5-30 minutes at direct current of 1-10 mA or at constant potential of 1-10 V.

EFFECT: invention enables to obtain titanium oxide nanoparticles in the form of nanospheres, nanofibres or nanorods depending on conditions of synthesis.

1 cl, 8 dwg, 7 ex

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RU 2 602 126 C2

Authors

Lebedeva Olga Konstantinovna

Kultin Dmitrij Jurevich

Root Natalja Viktorovna

Kustov Leonid Modestovich

Dzhungurova Giljana Evgenevna

Kalmykov Konstantin Borisovich

Dunaev Sergej Fedorovich

Dates

2016-11-10Published

2014-11-12Filed