FIELD: chemistry.
SUBSTANCE: invention can be used in producing heterogeneous catalysts with highly developed surface, and electrodes in lithium-ion batteries. Electrochemical method for producing nano-sized titanium (IV) oxide structures involves anodic oxidation of titanium electrode in ionic liquid with addition of water or propylene glycol in an air atmosphere. Ionic liquid has general formula K+A-, where K+ - alkylimideazoline, A- -NTf2 -, or PF6 -, or Cl-. Anodic oxidation is carried out at 20-25 °C for 5-30 minutes at direct current of 1-10 mA or at constant potential of 1-10 V.
EFFECT: invention enables to obtain titanium oxide nanoparticles in the form of nanospheres, nanofibres or nanorods depending on conditions of synthesis.
1 cl, 8 dwg, 7 ex
Title | Year | Author | Number |
---|---|---|---|
ELECTROCHEMICAL METHOD OF PRODUCING NANO-SIZED STRUCTURES OF NICKEL (II) OXIDE | 2015 |
|
RU2592892C1 |
ELECTRO-CHEMICAL PROCEDURE OF PRODUCTION OF METALLIC TUNGSTEN IN HIGH DISPERSED REACTIVE STATE | 2008 |
|
RU2408740C2 |
METHOD FOR PREPARING CATALYST FOR PRODUCTION OF SYNTHESIS GAS FROM METHANE, CATALYST PREPARED BY THIS METHOD AND METHOD OF PRODUCING SYNTHESIS GAS FROM METHANE WITH ITS USE | 2016 |
|
RU2638831C1 |
ELECTRO-CHEMICAL METHOD OF GRAPHENE OBTAINING | 2012 |
|
RU2500615C1 |
METHOD FOR PRODUCING PHOTOCATALYST BASED ON NANO-HETEROSTRUCTURAL SEMICONDUCTOR CdS-WO-TiO | 2016 |
|
RU2624620C1 |
ELECTROCHEMICAL METHOD OF PRODUCING TITANIUM DIBORIDE NANOPOWDERS | 2011 |
|
RU2465096C1 |
ANODE MATERIAL FOR LITHIUM-ION ACCUMULATOR AND METHOD OF ITS PRODUCTION | 2019 |
|
RU2703629C1 |
METHOD FOR ELECTROCHEMICAL DEPOSITION OF ACTINIDES | 2012 |
|
RU2493295C1 |
SOLID-OXIDANT FUEL CELL USING CERAMIC ANODE | 2003 |
|
RU2323506C2 |
METHOD FOR ELECTROCHEMICAL PRODUCTION OF GRAPHITE NANOPARTICLES | 2024 |
|
RU2823291C1 |
Authors
Dates
2016-11-10—Published
2014-11-12—Filed