FIELD: technological processes.
SUBSTANCE: invention relates to treating a zirconium containing feedstock. Method includes fluorinating a feedstock comprising dissociated zirconium, to obtain a zirconium fluorine compound and a silicon fluorine compound. Zirconium fluorine compound is separated from silicon fluoride compound. Method optionally includes reaction of zirconium fluorine compound with a halogen, alkali metal halide or alkali-earth metal halide to obtain zirconium halide. Method then includes plasma reduction of zirconium fluorine compound or, in case of presence thereof, zirconium halide in presence of a reducing agent to obtain zirconium metal.
EFFECT: method enables to produce nuclear-pure zirconium metal or zirconium metal with less rigid characteristics in terms of hafnium content; process is "dry", which enables to obtain less waste in comparison with a "wet" method.
13 cl, 1 dwg
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Authors
Dates
2017-02-06—Published
2012-10-11—Filed