METHOD FOR PRODUCTION OF LANTHANUM ORGANOMETALLIC FRAME COMPOUND OF THREE-DIMENSIONAL STRUCTURES BASED ON TEREPHTHALIC ACID Russian patent published in 2017 - IPC B01J23/00 B01J23/10 B01J27/20 B01J35/00 B01J37/00 

Abstract RU 2613976 C1

FIELD: chemistry.

SUBSTANCE: invention relates to the preparation of organometallic lanthanum frame compound of the formula La2(VDS)3(H2O)4 of a three-dimensional structure based on terephthalic acid, which can be used as a catalyst for various processes, including photocatalyst. The method for lanthanum organometallic frame compound preparation comprises terephthalic acid reaction with lanthanum nitrate for 8-9 hours at a temperature of 150-155°C in a solvent represented by dimethylformamide, reaction mixture coolong down to the room temperature, filtration of the resulting solid, successive washing of the solid phase by dimethylformamide and ethanol and drying at a temperature of 140-160°C.

EFFECT: simplified synthesis conditions, increased process efficiency and increased yield.

1 dwg, 1 tbl, 2 ex

Similar patents RU2613976C1

Title Year Author Number
METHOD OF A METAL-ORGANIC FRAME COMPOUND PRODUCTION WITH LUMINESCENT PROPERTIES 2016
  • Emelin Aleksej Vladimirovich
  • Rudakova Aida Vitalevna
  • Shurukhina Anna Vladimirovna
  • Maevskij Anton Vitalevich
  • Zharovov Dmitrij Anatolevich
RU2645513C1
METHOD OF MONOALCOHOL ALKOXYLATION IN PRESENCE OF METAL ORGANIC FRAME MATERIALS 2004
  • Mjuller Ul'Rikh
  • Metelkina Ol'Ga
  • Khesse Mikhaehl'
  • Shteser Mikhaehl'
  • Khaas Peter
  • Jagi Omar M.
RU2346925C2
METHOD OF PRODUCING MESOPOROUS CHROMIUM (III) TEREPHTHALATE 2011
  • Kovalenko Konstantin Aleksandrovich
  • Fedin Vladimir Petrovich
RU2457213C1
NEW HYBRID ORGANIC-INORGANIC MATERIAL IM-19 AND METHOD OF ITS PRODUCTION 2009
  • Shaple Zheral'
  • Simon-Masseron Anzhelik
  • Patarehn Zhoehl'
  • Ba Nikolja
  • Bazer-Bashi Dehl'Fin
RU2490059C2
ADSORBENT TO WITHDRAW HYDROCARBONS FROM AUTOMOTIVE EXHAUST GASES 2009
  • Kustov Leonid Modestovich
  • Kapustin Gennadij Ivanovich
  • Isaeva Vera Il'Inichna
  • Bogdan Viktor Ignat'Evich
RU2406558C1
METHOD OF OBTAINING TITANIUM-CONTAINING ORGANOMETALLIC CAGED COMPOUND 2013
  • Kudrik Evgenij Valentinovich
  • Makarova Anna Sergeevna
  • Makarov Sergej Vasil'Evich
  • Sal'Nikov Denis Sergeevich
  • Kojfman Oskar Iosifovich
RU2532554C1
METHOD OF PRODUCING POROUS COORDINATION POLYMERS MIL-53 2015
  • Tarasov Andrej Leonidovich
  • Isaeva Vera Ilinichna
  • Kustov Leonid Modestovich
RU2578600C1
FAST AND SCALABLE METHOD OF PRODUCING MICROPOROUS TEREPHTHALATE OF ZIRCONIUM (IV) 2019
  • Kovalenko Konstantin Aleksandrovich
  • Fedin Vladimir Petrovich
  • Sagidullin Aleksej Kausarovich
  • Orlioglo Bogdan Mikhajlovich
  • Bolotov Vsevolod Aleksandrovich
  • Knyazev Aleksej Sergeevich
  • Mazov Ilya Nikolaevich
  • Gorbin Sergej Igorevich
  • Malkov Viktor Sergeevich
RU2719597C1
ORGANOMETALLIC FRAMEWORK STRUCTURE OF LANTHANUM (III) BENZENE TRICARBOXYLATE La-BTC AND METHOD OF ITS MANUFACTURING 2022
  • Knyazeva Marina Konstantinovna
  • Shkolin Andrej Vyacheslavovich
  • Grinchenko Aleksandr Evgenevich
  • Solovtsova Olga Vyacheslavovna
  • Fomkin Anatolij Alekseevich
  • Menshchikov Ilya Evgenevich
  • Khozina Elena Vadimovna
RU2796682C1
GAS STORAGE DEVICE, METHOD OF GAS STORING, AGENT FOR ADSORPTION AND HOLDING OF METHANE, COMPLEX OF DICARBOZYLIC ACID WITH COPPER 1996
  • Masataka Fudzivara
  • Kendzi Seki
  • Vasuke Mori
  • Satosi Takamizava
RU2148204C1

RU 2 613 976 C1

Authors

Vlasova Elena Aleksandrovna

Makarova Anna Sergeevna

Maevskij Anton Vitalevich

Rudakova Aida Vitalevna

Makarov Sergej Vasilevich

Emelin Aleksej Vladimirovich

Kojfman Oskar Iosifovich

Dates

2017-03-22Published

2015-12-29Filed