METHOD OF PRODUCING MESOPOROUS CHROMIUM (III) TEREPHTHALATE Russian patent published in 2012 - IPC C07F11/00 

Abstract RU 2457213 C1

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing mesoporous chromium (III) terephthalate which can be used to produce heterogeneous catalysts. The method involves reaction of a mixture of chromium (III) nitrate and terephthalic acid in aqueous solution while heating. Heating is carried out in a closed volume at a rate of 1-1.5°/min to 220°C and the holding at that temperature for 6 hours. After cooling to room temperature, the obtained solid product is cleaned by successively treating with hot N,N-dimethylformamide and ethanol.

EFFECT: method enables to obtain mesoporous chromium (III) terephthalate with high content of mobile (labile) nitrate ions, which provides high sorption capacity of anionic complexes.

2 cl, 3 dwg, 1 ex

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RU 2 457 213 C1

Authors

Kovalenko Konstantin Aleksandrovich

Fedin Vladimir Petrovich

Dates

2012-07-27Published

2011-02-24Filed