FIELD: chemistry.
SUBSTANCE: to prepare silver nanoparticles, an aqueous stabiliser solution is first prepared. As a stabiliser, β-cyclodextrin or sodium bis (2-ethylhexyl) sulfosuccinate. Concentration β-cyclodextrin is in the range from 0.6⋅10-3 up to 1.2⋅10-3 M. The sodium concentration of bis (2-ethylhexyl) sulfosuccinate is in the range of 1.0⋅10-3 up to 3.0⋅10-3 M. Then, an aqueous alkaline solution of flavonoid quercetin is added to the stabiliser solution. To the resulting solution, with constant stirring, a solution of silver diamine nitrate is added to a predetermined molar concentration of 0.4⋅10-3 up to 4⋅10-3 M. The introduction of a solution of quercetin into the solution is carried out to a molar concentration of quercetin equal to 0.1 from the above molar concentration of silver diamine nitrate.
EFFECT: invention makes it possible to obtain nanoparticles with an average size of 14-16 nm, reduce the toxicity of solutions of silver nanoparticles for living organisms and increase the concentration of nanoparticles in solution.
5 cl, 9 dwg, 3 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD FOR MAKING METALLIC PARTICLES WITH NANOSTRUCTURE | 1999 |
|
RU2147487C1 |
METHOD OF PRODUCING SILVER NANOPARTICLES USING MODIFIED CHITOSAN | 2019 |
|
RU2701914C1 |
METHOD OF PRODUCING SILVER HYDROSOL | 2016 |
|
RU2638716C2 |
COLLOIDAL SOLUTION OF SILVER NANOPARTICLES, METAL-POLYMER NANOCOMPOSITE FILM MATERIAL, METHODS FOR PRODUCTION THEREOF, BACTERICIDAL COMPOSITION BASED ON COLLOIDAL SOLUTION AND BACTERICIDAL FILM MADE FROM METAL-POLYMER MATERIAL | 2011 |
|
RU2474471C2 |
METHOD FOR INCREASING THE QUANTITY AND ANTIBACTERIAL ACTIVITY OF SILVER NANOPARTICLES ON A SILK SUTURE MATERIAL | 2021 |
|
RU2770277C1 |
METHOD OF PRODUCING STABLE HIGH-CONCENTRATED ORGANOSOLS BASED ON SILVER NANOPARTICLES TO PRODUCE CONDUCTIVE FILMS | 2017 |
|
RU2644176C1 |
METHOD OF PRODUCING NANOPARTICLES OF NOBLE METALS USING BAZIDIAC MACROMYCETES | 2017 |
|
RU2679065C1 |
METHOD OF PRODUCING CERIUM OXIDE NANOPARTICLES | 2019 |
|
RU2698679C1 |
METHOD FOR PRODUCING COLLOIDAL SILVER SOLUTION | 2023 |
|
RU2806006C1 |
METHOD FOR OBTAINING A SOLUTION OF COLLOIDAL SILVER | 2020 |
|
RU2756226C1 |
Authors
Dates
2017-05-03—Published
2016-06-01—Filed