FIELD: chemistry.
SUBSTANCE: polyaminocarboxylates purification method comprises the following steps: a) processing aqueous polyaminocarboxylates inorganic acid, wherein the pH value of the solution is less than 0.75; b) recrystallizing the precipitated salt polyamino acid from water or aqueous solvent mixtures; c) treatment of an aqueous salt solution polyamino acid resin or a basic solution to maintain the pH at from 1.5 to 3.0; d) isolation of the pure polyaminocarboxylates as a chelating agent, wherein after step (a) above, the product is precipitated as a salt Polyamino acid; and wherein the precipitated salt Polyamino acid obtained in step (a) above, is isolated by filtration recrystallization before performing step (b).
EFFECT: increase the degree of purification.
9 cl, 2 ex
Title | Year | Author | Number |
---|---|---|---|
METHOD OF OBTAINING CHELATE COMPOUNDS | 2010 |
|
RU2533833C2 |
COMPOSITIONS OF METAL COMPLEXES | 2015 |
|
RU2710360C2 |
DIASTEREOISOMERICALLY ENRICHED COMPLEX OF GADOLINIUM AND CHELATING LIGAND BASED ON PCTA, METHOD FOR ITS PREPARATION AND PURIFICATION | 2020 |
|
RU2806027C2 |
METHODS FOR SYNTHESIS OF RADIONUCLIDE COMPLEX | 2019 |
|
RU2826739C2 |
COMPOSITIONS CONTAINING COMPLEXES OF METALS OF SERIES OF LANTHANIDES | 2015 |
|
RU2707070C2 |
METHOD OF Ga COMPLEXES PRODUCTION | 2012 |
|
RU2605090C2 |
DOTA SYNTHESIS | 2016 |
|
RU2730519C2 |
METHODS FOR PRODUCING RADIOIMMUNOCONJUGATES | 2010 |
|
RU2704802C2 |
METHOD FOR PRODUCING CALCOBUTROL | 2019 |
|
RU2779668C1 |
METHOD FOR PRODUCTION OF Ga COMPLEXES | 2012 |
|
RU2779132C2 |
Authors
Dates
2017-06-08—Published
2012-11-26—Filed