METHOD FOR PREPARING SULFOCATIONITES FROM HEAVY OIL RESIDUES Russian patent published in 2017 - IPC C08F8/36 C10C3/02 

Abstract RU 2623574 C1

FIELD: chemistry.

SUBSTANCE: method for preparing sulphocationites from heavy oil residues involves treating the feedstock with concentrated sulfuric acid with stirring, washing the desired product with water to remove excess sulfuric acid (pH 7), removing water and drying the desired product. According to the invention, heavy oil residues with a total content of asphaltene-resinous components of, at least, 50 wt %, which are pre-dissolved to a feed content of 10-20 wt %, sulfonation is carried out with a 4-6-fold excess of concentrated sulfuric acid at room temperature for, at least, 5 minutes, followed by centrifugation to isolate the desired product, which is carried out before removal of excess sulfuric acid.

EFFECT: method makes it possible to prepare sulphocathionites in a short time at room temperature based on heavy oil residues with good ion-exchange properties, while the amount of washing water necessary for washing the desired product is significantly reduced.

3 cl, 2 tbl, 8 ex

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RU 2 623 574 C1

Authors

Yakubov Makhmut Renatovich

Gryaznov Pavel Ivanovich

Yakubova Svetlana Gabidullinovna

Milordov Dmitrij Valerevich

Borisov Dmitrij Nikolaevich

Mironov Nikolaj Aleksandrovich

Sinyashin Kirill Olegovich

Dates

2017-06-28Published

2016-09-07Filed