FIELD: chemistry.
SUBSTANCE: invention relates to the field of organic chemistry, namely the method of obtaining salt 9-amino-10-methylacridinium of the overall formula I
,
where X=PF6 (connection a) X=ClO4 (connection b) X=BF4 (connection c), R=H, alkyl, interaction derived from dimedone aminering agent in a solvent that is different that as aminering agent using primary amine, solvent use acetonitrile, the reaction is carried out at room temperature and oxidation in electrochemically galvanostatic mode when current density 3 mA/cm2.
EFFECT: simple and secure way of getting salts 9-amino-10-methylacridinium, useful as raw material for the synthesis of a variety of compounds.
1 cl
| Title | Year | Author | Number |
|---|---|---|---|
| METHOD OF PRODUCING 9-MESITYL-10-METHYL ACRIDINIUM SALT | 2015 |
|
RU2582126C1 |
| ELECTROCHEMICAL METHOD FOR OBTAINING TETRAHYDROQUINOLINE DERIVATIVES, THEIR USE AS FUNGICIDAL AGENTS AND FUNGICIDAL COMPOSITIONS BASED ON THEM | 2022 |
|
RU2784323C1 |
| METHOD FOR ELECTROCHEMICAL STEREOSELECTIVE α-HYDROXYALKYLATION OF GLYCINE | 2014 |
|
RU2575710C1 |
| METHOD FOR PREPARING NITROSONIUM SALT | 0 |
|
SU1043184A1 |
| METHOD OF PRODUCING (4S)-4-(4-CYANO-2-METHOXYPHENYL)-5-ETHOXY-2,8-DIMETHYL-1,4-DIHYDRO-1,6-NAPHTHYRIDINE-3-CARBOXAMIDE AND ISOLATING (4S)-4-(4-CYANO-2-METHOXYPHENYL)-5-ETHOXY-2,8-DIMETHYL-1,4-DIHYDRO-1,6-NAPHTHYRIDINE-3-CARBOXAMIDE BY ELECTROCHEMICAL METHODS | 2016 |
|
RU2715226C2 |
| ELECTROCHEMICAL METHOD FOR SYNTHESIS OF ORGANONICKEL SIGMA-COMPLEXES | 2009 |
|
RU2396375C1 |
| ELECTROCHEMICAL METHOD OF PRODUCING CHROMIUM 2-ETHYLHEXANOATE-PRECATALYST FOR TRIMERISATION OF ETHYLENE TO HEXENE-1 | 2023 |
|
RU2822543C1 |
| METHOD OF PRODUCING DIALKYL-(ARYL)TRIFLUORPHOSPHORANES | 0 |
|
SU1012580A1 |
| PROCESS FOR PREPARATION OF N-[(3-AMINOOXETAN-3-YL)METHYL]-2-(1,1-DIOXO-3,5-DIHYDRO-1,4-BENZOTHIAZEPINE-4-YL)-6-METHYL-QUINAZOLINE-4-AMINE | 2015 |
|
RU2664643C2 |
| METHOD OF SYNTHESIS OF PHOSPHORIC ACID ESTERS | 2001 |
|
RU2199545C1 |
