METHOD OF PRODUCING (4S)-4-(4-CYANO-2-METHOXYPHENYL)-5-ETHOXY-2,8-DIMETHYL-1,4-DIHYDRO-1,6-NAPHTHYRIDINE-3-CARBOXAMIDE AND ISOLATING (4S)-4-(4-CYANO-2-METHOXYPHENYL)-5-ETHOXY-2,8-DIMETHYL-1,4-DIHYDRO-1,6-NAPHTHYRIDINE-3-CARBOXAMIDE BY ELECTROCHEMICAL METHODS Russian patent published in 2020 - IPC C07D471/04 C25B3/04 

Abstract RU 2715226 C2

FIELD: chemistry.

SUBSTANCE: invention relates to a method of producing a compound of formula (I) and ent- (I) by electrochemical reduction of compounds of formulas (XVII), or M1a (S), or M1b (R), or a mixture of M1a (S) and M1b (R). Invention also relates to methods of producing compounds of formulas (XVII), M1a (S) and M1b (R).

EFFECT: technical result is a method of producing a compound of formula (I), characterized by high output and purity.

8 cl, 9 dwg, 3 tbl, 32 ex

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RU 2 715 226 C2

Authors

Plattsek, Jokhannes

Gottfrid, Katrin

Assmann, Jens

Lolli, Dzhulio

Dates

2020-02-26Published

2016-08-18Filed